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Solvent Recovery
DMF/DMAC Recovery System
 
Mitsubishi Rayon Engineering (MRE) has extensive experience in the recovery of solvents, undertaken in acrylic fiber plant operations for its parent company Mitsubishi Rayon. MRE hopes to fulfil your solvent-recovery needs and contribute to the realization of an increasingly recycling-oriented society. Having recorded the best performance in Japan with our DMF/DMAC recovery system, we are making utmost efforts to conserve natural resources through the recovery of resources.
Business field Solvent
Synthetic fiber DMF Acrylnitril
Synthetic leather DMAC Amino acid
Electronic materials MEK Acetic acid
Resin MIBK Formic acid
Agricultural chemicals Methylene chloride IQ
Coatings Acetone  
Pharmaceuticals Methanol  
Inorganic chemicals Ethanol  
Organic chemicals Toluene  
Overview of our DMF (Dimethyl Formamide)
recovery system
 
Characteristics
High recovery rate (99% or higher)
Recovery of high-purity DMF
Energy efficient
Compact
Reduces the environmental burden posed by discharged effluent
Condensation is possible in pre-treatment stages (utilizing membranes)
Long-term, continuous and stable operation
Easy maintenance
More than 40 orders received worldwide
 
Operation Flow
Solids removal process -- using unique MRE-designed pan dryer
Dehydration process -- MRE's Two-Column system
Formic acid removal process -- Formic acid density reduced to less than 50ppm
Formic acid decomposition process -- Formic acid decomposer
Operation Flow
 
Estimated cost-savings afforded by our solvent recovery system (assuming: continuous operation at 2 tons per hour of
DMF 10% solution)
Construction costs: ¥250 million
Operating costs: ¥104 million/year (including utilities and labor costs)
Value of recovered DMF: ¥235 million/year
  Period required for recovery of the initial costs: 250/(235-104)= 1.9 years
 
Facilities equipped with MRE's DMF/DMAC Recovery System
 
Company A Company B Company C
 
DMF quality standards and quality of recovered DMF
 
Item

Standard Recovered material
quality
JIS Class Mitsubishi Rayon Design values Actual results
Specific gravity
(25 centigrade)
0.949 ~ 0.954 (25 centigrade)
0.9435 ~ 0.9450
  (0.944)
Refractive index
(n 20D)
1.428
~ 1.432
(25 centigrade)
1.4275
~ 1.4290
  (1.429)
Reservoir (vol%) (151 ~ 154 centigrade) 95 or greater (151 ~ 155 centigrade) 98 or greater  
99 or greater
Water solution Within limits      
Ethanol solution Within limits      
Water content(%) Less than 0.2 Less than 0.05 Less than 0.02 0.005
~ 0.02
Non-volatile content (%) Less than 0.01      
Free acid (%) Less than 0.003   Less than 0.005 0.0004
~ 0.0012
Hue (APHA)   Less than 10   Less than 15 (determined at 15)
Total alkali (%)   Less than 0.005 Less than 0.005 0.0003
~ 0.0014
ph (20% water solution)   6.5 ~ 8.5 6.5 ~ 9.0 6.5 ~ 9.0
Iron (ppm)   Less than 0.03 Less than 0.05 Less than 0.025
Relative conductivity   Less than 3.0   0.2 ~ 2.2
 
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